Full Report Set



  ASAP 2020 V3.01 H    Unit 1    Serial #: 220    Page  1  

     Sample:    SJO113-3                          
   Operator:                                      
  Submitter:                                      
       File:    C:\2020\DATA\DUMELE\SJO113-3.SMP  

            Started:    16.03.2022 8:46:32        Analysis Adsorptive:    N2                    
          Completed:    18.03.2022 6:20:55        Analysis Bath Temp.:    -195.526 C           
        Report Time:    18.03.2022 15:59:55        Thermal Correction:    No                    
        Sample Mass:    0.0383 g                      Warm Free Space:    16.2424 cm Measured  
    Cold Free Space:    49.7928 cm            Equilibration Interval:    45 s                  
  Low Pressure Dose:    0.5000 mmol/g                 Automatic Degas:    No                    







                      Isotherm Tabular Report

   Relative       Absolute      Quantity    Elapsed    Saturation   
   Pressure       Pressure      Adsorbed     Time       Pressure    
    (p/p)         (mbar)       (mmol/g)    (h:min)      (mbar)     
-----
  1.#QNAN0000       1.#QNAN0     1.#QNAN      01:04    1036.986819  
  0.000011072       0.011484     0.50742      01:56       1.#QNAN0  
  0.000006313       0.006549     1.01711      02:41       1.#QNAN0  
  0.000004444       0.004611     1.52661      03:27       1.#QNAN0  
  0.000008140       0.008447     2.03457      04:15       1.#QNAN0  
  0.000017919       0.018600     2.53896      05:13       1.#QNAN0  
  0.000040414       0.041967     3.03507      06:57       1.#QNAN0  
  0.000087275       0.090709     3.51400      10:44       1.#QNAN0  
  0.000187568       0.195220     3.97015      16:40       1.#QNAN0  
  0.000373109       0.388866     4.36031      22:32       1.#QNAN0  
  0.000968304       1.010616     4.84661      28:32       1.#QNAN0  
  0.002211414       2.310701     5.28815      33:27       1.#QNAN0  
  0.004499262       4.705319     5.67572      37:08       1.#QNAN0  
  1.#QNAN0000       1.#QNAN0     1.#QNAN      37:15    1045.826263  
  0.008029506       8.398844     5.97511      38:10       1.#QNAN0  
  0.012508549      13.084262     6.18024      38:19       1.#QNAN0  
  1.#QNAN0000       1.#QNAN0     1.#QNAN      38:22    1046.034905  
  0.014779365      15.460257     6.26724      38:27       1.#QNAN0  
  0.015978275      16.715424     6.32097      38:36       1.#QNAN0  
  0.017533130      18.342384     6.36431      38:39       1.#QNAN0  
  0.020438784      21.383167     6.45228      38:46       1.#QNAN0  
  0.021089137      22.064170     6.47371      38:50       1.#QNAN0  
  0.023889885      24.995595     6.54763      38:57       1.#QNAN0  
  0.026851268      28.095378     6.62174      39:04       1.#QNAN0  
  0.030380818      31.790191     6.69715      39:12       1.#QNAN0  
  0.034793712      36.409037     6.76553      39:17       1.#QNAN0  
  0.039347853      41.176845     6.85010      39:25       1.#QNAN0  
  1.#QNAN0000       1.#QNAN0     1.#QNAN      39:28    1046.503942  
  0.045313241      47.420921     6.93160      39:31       1.#QNAN0  
  0.051182476      53.564140     7.00556      39:37       1.#QNAN0  
  0.052036247      54.458140     7.02248      39:40       1.#QNAN0  
  0.052925439      55.389226     7.03526      39:43       1.#QNAN0  
  0.053803846      56.308869     7.05184      39:45       1.#QNAN0  
  0.054841433      57.395292     7.06702      39:48       1.#QNAN0  
  0.055737799      58.333936     7.08387      39:51       1.#QNAN0  
  0.056960956      59.614613     7.09778      39:54       1.#QNAN0  
  0.058402974      61.124372     7.11525      39:57       1.#QNAN0  
  0.059821615      62.609693     7.13572      40:00       1.#QNAN0  
  0.061561621      64.431189     7.15122      40:02       1.#QNAN0  
  0.063346806      66.299993     7.16793      40:04       1.#QNAN0  
  0.065205640      68.246112     7.18495      40:07       1.#QNAN0  
  0.067141859      70.273046     7.20200      40:09       1.#QNAN0  
  0.068976735      72.193934     7.21564      40:11       1.#QNAN0  
  0.071158073      74.477698     7.23503      40:14       1.#QNAN0  
  0.073380027      76.804014     7.25333      40:17       1.#QNAN0  
  0.075464154      78.985873     7.26947      40:19       1.#QNAN0  
  0.080329041      84.078564     7.29977      40:22       1.#QNAN0  
  0.085988926      90.003463     7.33512      40:25       1.#QNAN0  
  0.097605100     102.162897     7.39038      40:28       1.#QNAN0  
  1.#QNAN0000       1.#QNAN0     1.#QNAN      40:31    1046.705911  
  0.100291925     104.978309     7.42323      40:33       1.#QNAN0  
  0.111353133     116.561171     7.47290      40:37       1.#QNAN0  
  0.126630391     132.557041     7.53040      40:40       1.#QNAN0  
  0.140542942     147.125274     7.58597      40:43       1.#QNAN0  
  0.144302562     151.065635     7.60388      40:46       1.#QNAN0  
  0.163980486     171.671102     7.66078      40:49       1.#QNAN0  
  0.186508816     195.262023     7.71859      40:52       1.#QNAN0  
  0.212049285     222.007998     7.77510      40:55       1.#QNAN0  
  0.241315384     252.656343     7.83176      40:58       1.#QNAN0  
  0.250759210     262.549392     7.86209      41:00       1.#QNAN0  
  0.274724298     287.650137     7.89767      41:03       1.#QNAN0  
  0.300447753     314.590351     7.92963      41:05       1.#QNAN0  
  0.312254550     326.962994     7.96237      41:08       1.#QNAN0  
  0.350284956     366.796092     7.98828      41:11       1.#QNAN0  
  0.373628132     391.247619     8.01179      41:13       1.#QNAN0  
  0.400374318     419.263713     8.02902      41:15       1.#QNAN0  
  0.422586013     442.532435     8.04848      41:17       1.#QNAN0  
  0.450315302     471.585106     8.06507      41:20       1.#QNAN0  
  0.478275227     500.875958     8.08053      41:22       1.#QNAN0  
  0.500051633     523.692161     8.09702      41:24       1.#QNAN0  
  0.523345258     548.098281     8.11091      41:26       1.#QNAN0  
  0.549970759     576.000860     8.12685      41:29       1.#QNAN0  
  0.595531681     623.730995     8.13731      41:31       1.#QNAN0  
  1.#QNAN0000       1.#QNAN0     1.#QNAN      41:33    1047.373011  
  0.618059812     647.350233     8.17950      41:36       1.#QNAN0  
  0.650552876     681.390939     8.19505      41:38       1.#QNAN0  
  0.696243463     729.259857     8.21406      41:41       1.#QNAN0  
  0.718441326     752.518936     8.23902      41:43       1.#QNAN0  
  0.740397385     775.525269     8.26039      41:45       1.#QNAN0  
  0.773881896     810.607678     8.29935      41:47       1.#QNAN0  
  0.807373550     845.703189     8.36762      41:50       1.#QNAN0  
  0.873793508     915.292046     8.63233      41:53       1.#QNAN0  
  0.914139445     957.575932     9.02403      41:57       1.#QNAN0  
  0.926204380     970.225204     9.23270      41:59       1.#QNAN0  
  0.947084745     992.126240     9.73113      42:04       1.#QNAN0  
  0.953319838     998.669242     9.97183      42:06       1.#QNAN0  
  0.984446007    1031.340716    12.62889      42:17       1.#QNAN0  
  0.993486148    1040.876718    15.44661      42:28       1.#QNAN0  
  0.982175710    1029.061932    14.12249      42:34       1.#QNAN0  
  1.#QNAN0000       1.#QNAN0     1.#QNAN      42:36    1047.749038  
  0.971777680    1018.256177    12.60622      42:43       1.#QNAN0  
  0.962119952    1008.223715    11.53589      42:51       1.#QNAN0  
  0.960557731    1006.619273    11.32432      42:54       1.#QNAN0  
  0.948670350     994.226328    10.53974      43:00       1.#QNAN0  
  0.933966181     978.868945     9.92698      43:05       1.#QNAN0  
  0.918204080     962.390641     9.50744      43:09       1.#QNAN0  
  0.899329440     942.648445     9.18432      43:13       1.#QNAN0  
  0.873755398     915.872239     8.92898      43:16       1.#QNAN0  
  0.843100177     883.768020     8.74910      43:19       1.#QNAN0  
  0.822250316     861.940383     8.66851      43:22       1.#QNAN0  
  0.801984967     840.714991     8.61492      43:24       1.#QNAN0  
  0.781813344     819.595792     8.58138      43:27       1.#QNAN0  
  0.770096926     807.330603     8.56287      43:29       1.#QNAN0  
  0.739644269     775.430713     8.53742      43:32       1.#QNAN0  
  0.700074952     733.962759     8.51976      43:34       1.#QNAN0  
  0.649686028     681.156787     8.53786      43:37       1.#QNAN0  
  1.#QNAN0000       1.#QNAN0     1.#QNAN      43:39    1048.462603  
  0.581078993     609.254969     8.57876      43:41       1.#QNAN0  
  0.531281157     557.063570     8.61941      43:44       1.#QNAN0  
  0.481403805     504.778470     8.64914      43:46       1.#QNAN0  
  0.431311476     452.271016     8.67105      43:49       1.#QNAN0  
  0.381342210     399.883589     8.70536      43:51       1.#QNAN0  
  0.331316423     347.438630     8.72761      43:54       1.#QNAN0  
  0.281348196     295.046341     8.74032      43:56       1.#QNAN0  
  0.231485271     242.764902     8.72321      43:59       1.#QNAN0  
  0.200372536     210.144083     8.69139      44:02       1.#QNAN0  
  0.150633142     157.989017     8.60246      44:07       1.#QNAN0  
  0.100938476     105.876958     8.40739      44:14       1.#QNAN0  
  0.070187365      73.630614     8.19276      44:24       1.#QNAN0  
  0.028607187      30.018923     7.58770      44:46       1.#QNAN0  
  1.#QNAN0000       1.#QNAN0     1.#QNAN      44:49    1049.388715  
  0.009539259      10.010390     6.84517      45:09       1.#QNAN0  




 Options Report


              Sample Tube

         Warm freespace:    1.0000 cm  
         Cold freespace:    1.0000 cm  
    Non-ideality factor:    0.0000620   
  Use Isothermal Jacket:    Yes         
         Use Filler Rod:    Yes         
       Vacuum seal type:    Seal Frit   

 Analysis Conditions


                 Preparation

               Fast evacuation:    No        
  Unrestricted evacuation from:    6.7 mbar  
               Vacuum setpoint:    13 bar   
               Evacuation time:    0.10 h    
                     Leak test:    No        
                 Use TransSeal:    No        

                Free Space

             Free-space type:    Measured  
  Lower dewar for evacuation:    Yes       
             Evacuation time:    0.10 h    
                 Outgas test:    No        

                                                       p and Temperature

         p and T type:    Measure p at intervals during analysis.  Calculate the Analysis Bath Temperature from these values.  
  Measurement interval:    60 min                                                                                                

                         Dosing

  Use first pressure fixed dose:    No                  
   Use maximum volume increment:    No                  
               Target tolerance:    5.0% or 6.666 mbar  
            Low pressure dosing:    Yes                 
                    Dose amount:    0.50000 mmol/g      
    Minimum equilibration delay:    0.00 h              
    Maximum equilibration delay:    999.00 h            

                      Equilibration

       Equilibration time (p/p = 0.010000000):    45 s   
       Equilibration time (p/p = 1.000000000):    10 s   
  Minimum equilibration delay at p/p >= 0.995:    600 s  

             Sample Backfill

  Backfill at start of analysis:    Yes  
    Backfill at end of analysis:    Yes  
                   Backfill gas:    N2   

                Adsorptive Properties

                         Adsorptive:    Nitrogen      
          Maximum manifold pressure:    1233.23 mbar  
                Non-ideality factor:    0.0000620     
          Density conversion factor:    0.0015468     
  Therm. tran. hard-sphere diameter:    0.386 nm      
     Molecular cross-sectional area:    0.162 nm     


  Inside diameter of sample tube:    9.53 mm  

